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Features of crystallization of the eutectic alloy in the gallium-indium system

V. D. AleksandrovDonbas National Academy of Civil Engineering and ArchitectureS. A. FrolovaDonbas National Academy of Civil Engineering and ArchitectureD. A. ShkilniukDonbas National Academy of Civil Engineering and ArchitectureD. V. MaltsevDonbas National Academy of Civil Engineering and Architecture
Annotation: The method of cyclic thermal analysis was used to study the effect of overheating of the melt of the eutectic alloy Ga + 14.2 mol% In on the value of precrystallization supercooling on samples weighing 2 g. It has been established that when superheating a liquid eutectic is higher than the eutectic temperature TE = 288.3 K and subsequent cooling, the dependence of supercooling from overheating has a monotonically increasing character. The limiting value of supercooling is 25 K after preliminary heating of the melt to 400 K. It has been established that crystallization from a supercooled state was always “explosive” at a rate of ≈40-45 K / s. In this case, neither the cooling rate from 0.01 to 10 K / s nor the long-term (for several hours) isothermal exposure of the melt in superheated and supercooled conditions affected the magnitude of supercooling.

Keywords: gallium, indium, eutectic alloy, thermal analysis, overheating, pre-crystallization supercooling, extreme supercooling.

Pages: 73-75.

PDF

For citation: Aleksandrov, V. D.; Frolova, S. A.; Shkilniuk, D. A. [et al.]. Features of crystallization of the eutectic alloy in the gallium-indium system. – Text : direct. – In: The Builder of Donbass. – 2019. – Issue 4-2019. – Р. 73-75. – ISSN 2617-1848.


Issue Cover
Issue 4-2019
Journal: The Builder of Donbass
Publish house: Donbas National Academy of Civil Engineering and Architecture